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Journal Articles

Assembly of the US-Japan MFE-RB-15J experiment for irradiation in the HFIR

Hirose, Takanori; Ando, Masami; Tanigawa, Hiroyasu; Okubo, Nariaki; McDuffee, J. L.*; Heatherly, D. W.*; Sitterson, R. G.*; Stoller, R. E.*; Yamamoto, Takuya*

Fusion Materials Semiannual Progress Report (DOE/ER-0313/46) (Internet), p.72 - 78, 2009/06

This work is being carried out under Annex I of the collaboration on Fusion Materials between the U.S. DOE and the Japan Atomic Energy Agency. The MFE-RB-15J capsule is a part of the Phase-V experiments with the goal of elucidating the effects of helium in fusion structural candidate engineering alloys, and verifying the irradiation response of alloy F82H and its joint for ITER-TBM (Test Blanket Module) application. The target dose of this capsule is 6 dpa at the peak and it will introduce 300 appm of transmutation helium in F82H with additional boron-10. Assembly of the MFE-RB-15J capsule was completed on April, 2008. Irradiation began for MFE-RB-15J with cycle 415, starting June 3, 2008. The MFE-RB-15J experiment was installed in location RB-1A with europium thermal neutron shield. A detailed specimen loading list for the capsule is provided in this report.

Journal Articles

Mechanical properties and microstructural stability of advanced ferritic/martensitic steel under irradiation

Yano, Yasuhide; Yamashita, Shinichiro; Akasaka, Naoaki; Watanabe, Seiichi*; Takahashi, Heishichiro

Proceedings of 9th China-Japan Symposium on Materials for Advanced Energy Systems and Fission & Fusion Engineering jointed with CAS-JSPS Core-university Program Seminar on Fusion Materials, System and Design Integration, p.2 - 5, 2007/10

Ferritic/martensitic (F/M) steels are expected to be prospective not only for the long life core material of fast reactors but also for the blanket materials of fusion reactor because of their superior swelling resistance. Japan Atomic Energy Agency has developed a 11Cr-0.5Mo-2W-V, Nb F/M steel (PNC-FMS) for core materials of next fast reactor. In order to evaluate the effect of structural change due to irradiation on mechanical properties of PNC-FMS, neutron irradiations were carried out between 773 and 1013 K to doses of from 11 to 102 dpa in JOYO reactor. Post irradiation tensile tests were performed at 773-1013 K with a strain rate of 0.5$$times$$10$$^{-4}$$/s. The stability of microstructures under irradiation was also compared with those of electron irradiation using HVEM.

Journal Articles

Effects of irradiation and water temperatures on IASCC susceptibility of stainless steels

Miwa, Yukio; Tsukada, Takashi

Proceedings of 8th Japan-China Symposium on Materials for Advanced Energy Systems and Fission & Fusion Engineering, p.161 - 168, 2004/10

Irradiation assisted stress corrosion cracking (IASCC) is one of the environmental degradation problems of in-core structural materials for light water reactors. The effects of irradiation and water temperatures on the IASCC were studied using type 316(LN) stainless steels irradiated at 333-673 K to 1.1-16 dpa. IASCC did not occur at 513 K in oxygenated water for specimens irradiated below 573 K to 1.1-16 dpa, but IASCC occurred above 533 K in oxygenated water for all specimens. The irradiation temperature had a strong influence on IASCC susceptibility at 513 K in oxygenated water, so that the irradiation temperature dependence was compared with the temperature dependence of other radiation-induced phenomena.

Journal Articles

Analysis of Ta-rich MX precipitates in RAFs

Tanigawa, Hiroyasu; Sakasegawa, Hideo*; Hashimoto, Naoyuki*; Zinkle, S. J.*; Klueh, R. L.*; Koyama, Akira*

Fusion Materials Semiannual Progress Report for the Period Ending (DOE/ER-0313/35), p.33 - 36, 2004/04

Extraction replica samples were prepared from F82H-IEA, F82H HT2, JLF-1 and ORNL9Cr to analyze the precipitate distribution. The samples were examined to obtain precipitate size distribution with TEM and to analyze chemical composition distribution with SEM. Back-scattered electron imaging was found to be the effective way to separate Ta-rich precipitate from other precipitates. Results showed that most of the precipitates were M23C6, and the shape is a round ellipsoid in F82H-IEA and HT2, but was a long ellipsoid in JFL-1 and ORNL9Cr. It was also found that MX precipitates were few and large and contain Ti in F82H-IEA and HT2, but a lot of fine MX precipitates without Ti were observed in JLF-1 and ORNL9Cr.

Journal Articles

Analysis of extraction residue of HFIR 11J-irradiated RAFs

Tanigawa, Hiroyasu; Sakasegawa, Hideo*; Zinkle, S. J.*; Klueh, R. L.*; Koyama, Akira*

Fusion Materials Semiannual Progress Report for the Period Ending (DOE/ER-0313/35), p.30 - 32, 2004/04

Extraction residue was made from several HFIR 11J-irradiated RAFs, and the mass change was measured to investigate the irradiation-enhanced change in precipitation. Two different types of filter with coarse and fine pores were used in order to separate the difference of irradiation effects between larger and smaller precipitates. Unirradiated specimens were examined as well. Results suggest that during irradiation the mass of larger precipitates increased in F82H-IEA, Ni-doped F82H, JLF-1 and ORNL9Cr, fine precipitates disappeared in JLF-1, and fine precipitates increased in Ni-doped F82H.

Journal Articles

X-ray diffraction analysis on precipitates of 11J irradiated RAFs

Tanigawa, Hiroyasu; Sakasegawa, Hideo*; Payzant, E. A.*; Zinkle, S. J.*; Klueh, R. L.*; Koyama, Akira*

Fusion Materials Semiannual Progress Report for the Period Ending (DOE/ER-0313/35), p.37 - 40, 2004/04

XRD analyses were performed on the extraction residue of HFIR 11J-irradiated RAFs to investigate the overall precipitate character. Un-irradiated and aged specimens were examined as well. Results suggested that the distinctive peaks of M23C6 (M; Cr, Fe, W) were observed on all specimens. Peaks possibly related to MX (M;Ta,Ti,V : X ; C, N) were observed on the specimens extracted from un-irradiated JLF-1 and ORNL9Cr, but those peaks were not observed on irradiated specimens.

Journal Articles

On the effects of fatigue precracking on the microstructure around precrack in 1TCT fracture toughness specimen of F82H-IEA

Tanigawa, Hiroyasu; Hashimoto, Naoyuki*; Sokolov, M. A.*; Klueh, R. L.*; Ando, Masami

Fusion Materials Semiannual Progress Report for the Period Ending (DOE/ER-0313/35), p.58 - 60, 2004/04

1TCT fracture toughness specimens of F82H-IEA steel were fatigue precracked and sliced in specimen thickness wise for microstructure analysis around the precrack. The microstructure around the precrack was observed by optical microscopy (OM), scanning electron microscopy (SEM), orientation imaging microscopy (OIM), and transmission electron microscopy (TEM). TEM samples around the crack front were prepared by focused ion beam (FIB) processor. The fracture surfaces of tested 1TCT specimens were also observed. OM observation showed that the precrack penetration was straight in the beginning, and then tended to follow a prior austenite grain boundary and to branch into 2 to 3 directions at the terminal. SEM and OIM observations revealed that the both microstructures around the precracks and ahead of the precrack had turned into cell structure, which is the typical microstructure of fatigue-loaded F82H. TEM images and inverse pole figures obtained from the crack-front region confirmed this structure change.

Journal Articles

Development of two-step softening heat-treatment for manufacturing 12Cr-ODS ferritic steel tubes

Narita, Takeshi; Ukai, Shigeharu; Kaito, Takeji; Otsuka, Satoshi; Kobayashi, Toshimi*

Proceedings of 11th International Conference on Fusion Reactor Materials (ICFRM-11), 41(10), 0 Pages, 2004/00

Focusing on the cover layer materials (as the Radon Barrier Materials), which could have the effect to restrain the radon from scattering into the air and the effect of the radiation shielding, we produced the radon barrier materials with crude bentonite on an experimental basis, using the rotary type comprehensive unit for grinding and mixing, through which we carried out the evaluation of the characteristics thereof.

Journal Articles

Welding Technology Development in 9Cr-ODS Martensitic Steels

Seki, Masayuki; ; Ukai, Shigeharu; Kaito, Takeji; Hirako, Kazuhiko*

Proceedings of 11th International Conference on Fusion Reactor Materials (ICFRM-11), 87 Pages, 2003/00

None

Journal Articles

Microstructural changes of neutron irradiated ODS ferritic and martemsitic steels

Akasaka, Naoaki; Yamashita, Shinichiro; Yoshitake, Tsunemitsu; Ukai, Shigeharu; Kimura, Akihiko*

Proceedings of 11th International Conference on Fusion Reactor Materials (ICFRM-11), 0 Pages, 2003/00

Focusing on the cover layer materials (as the Radon Barrier Materials), which could have the effect to restrain the radon from scattering into the air and the effect of the radiation shielding, we produced the radon barrier materials with crude bentonite on an experimental basis, using the rotary type comprehensive unit for grinding and mixing, through which we carried out the evaluation of the characteristics thereof.

Journal Articles

Neutron irradiation response of B2-type ordered alloys

Hoshiya, Taiji; Takaya, Shigeru; Nakagiri, Toshio; Aoto, Kazumi

Proceedings of 11th International Conference on Fusion Reactor Materials (ICFRM-11), 0 Pages, 2003/00

Neutron irradiation response of a B2-type ordered alloy was obtained from the irradiation diagram. Two conflicting processes; irradiation disordering and ordering take place under irradiation and that state is decribed by the degree of Bragg-Williams's long range order and Warren-Cowley's short range order. The irradiated state reveals a function of temperature and dose rate and also, the first threshold value and the second threshold value were obtained at which the degree of order abruptly or gradually fall down, respectively. Our proposed irradiation diagram can be useful to judge the new material to be irradiation-resistant or not.

Journal Articles

Burst properties of imadiated oxide dispersion strengthened ferritic steel claddings

Yoshitake, Tsunemitsu; ; Miyakawa, Shunichi

10th International Conference on Fusion Reactor Materials, 154 Pages, 2001/00

None

Journal Articles

Journal Articles

Heavy irradiation effects in boron carbide

; Donomae, Takako; *

Heavy irradiation ef, 0 Pages, 2001/00

None

Journal Articles

High Temperature Capability of ODS Martensitic Steel Claddings

; Mizuta, Shunji; Yoshitake, Tsunemitsu; *

The Sixth Japan-China Symposium on Materials for Advanced Energy Systems and Fission & Fusion Engine, 0 Pages, 2001/00

None

Journal Articles

Tensile results of low-activation martensitic steel irradiated in HFIR RB-11J and RB-12J spectrally tailored capsules

Shiba, Kiyoyuki; Klueh, R. L.*; Miwa, Yukio; Igawa, Naoki; Robertson, J. P.*

Fusion Materials Semiannual Progress Report (DOE/ER-0313/28), p.131 - 135, 2000/06

no abstracts in English

Journal Articles

Microstructural evolution of cold-worked austenitic stainless steels irradiated to 17 DPA in spectrally tailored experiments of the ORR and HFIR at 400$$^{circ}$$C

Wakai, Eiichi; Hashimoto, N.*; J.P.Robertson*; Sawai, Tomotsugu; Hishinuma, Akimichi

Fusion Materials, 313(25), p.197 - 201, 1999/04

no abstracts in English

Journal Articles

Hydrogen production effect on microstructure of HFIR; Irradiated low activation F82H steel using $$^{54}$$Fe isotope

Wakai, Eiichi; Hashimoto, N.*; Shiba, Kiyoyuki; Miwa, Yukio; J.P.Robertson*; R.L.Klueh*

Fusion Materials, 313(25), p.151 - 160, 1999/04

no abstracts in English

Journal Articles

Swelling of HFIR-irradiated F82H, F82H+$$^{10}$$B and F82H+$$^{58}$$Ni steels

Wakai, Eiichi; Hashimoto, N.*; Shiba, Kiyoyuki; Miwa, Yukio; J.P.Robertson*; R.L.Klueh*

Fusion Materials, 313(25), p.161 - 169, 1999/04

no abstracts in English

Journal Articles

Irradiation Creep of 11Cr-0.5Mo-2W,V,Nb Ferritic-Martensitic,Modified 316,and 15Cr-20Ni Austenitic S.S.Irradiated in FFTF to 103-206 dpa

; Mizuta, Shunji;

9th International Conference on Fusion Reactor Materials, 195 Pages, 1999/00

None

32 (Records 1-20 displayed on this page)